Semiconductors are materials whose electrical conductivity lies between that of conductors (which readily allow the flow of electricity) and insulators (which resist the flow of electricity). Integrated circuits composed of numerous transistors and diodes, fabricated from semiconductor materials, are commonly referred to as semiconductors or semiconductor chips. Semiconductors are widely utilized in a broad range of applications, from home appliances and automobiles to critical social infrastructure.
Within the field of semiconductors, new materials such as SiC and GaN, advanced transistor structures, and cutting-edge 3D packaging technologies are receiving a significant attention for achieving lower power consumption and higher performance. To ensure high manufacturing yield and device reliability, precise characterization techniques and the appropriate selection of preprocessing and analytical instruments are essential. This page introduces various analytical instruments and application examples, highlighting their use in semiconductor manufacturing and research.
1. JEOL's Instruments Contributing to Semiconductor Inspection and Analysis
2. JEOL Semiconductor-Related Products and Their Applications
3. FIB-SEM/TEM: Application of TEM-Based CD Measurement in Advanced Semiconductor Processes
TEM-LINKAGE
JEOL adopts a double tilt cartridge that facilitates integration with the TEM. This cartridge is easily mounted onto a double-tilt TEM holder, eliminating any need to remove or exchange the FIB grid.
The figures below show a HAADF-STEM image of a Fin Field-Effect Transistor (FinFET) and a TEM image of a flash memory, both acquired using the JEM-ACE200F. Multi Image Tool developed by SYSTEM IN FRONTIER INC. is used for the measurement, enabling operators to create customized measurement recipes.
Creating a TEM Specimen of a FinFET
The figures on the left are an SE and BSE image of a FinFET. You can capture high-contrast images to target processing end points.
The FIB-SEM is capable of precisely thinning the Fin section region of interest. Using the DT transfer cartridge, you can move the specimen into a double tilting TEM holder for high resolution observation.
Structural and Compositional Analysis of FinFET
The figures on the left show an HAADF-STEM image and EDS maps of a FinFET. The shape of the FinFET, the structure around the gate, the arrangement of the contact region, and the elemental distribution can be clearly observed. In particular, the HAADF-STEM image provides a clear view of the gate insulating films (SiO2 and HfO2) as well as the layer structure of the metal gate.
Specimen: FinFET with a process rule of 5 nm
Accelerating voltage: 200 kV
EDS maps (net count maps)
4. SEM: SEM Functions for Observing and Analyzing Semiconductor Devices
A SEM is an instrument that scans the specimen surface with a fine electron beam to observe it. By leveraging attachments, such as EDS, CL, and Raman, various information, such as elemental analysis, crystal defects observation, and stress measurements, can be obtained.
The JSM-IT810 is equipped with Neo Engine, a next-generation electron optical control system, and SEM Center, which offers highly user-friendly operation, such as Zeromag and EDS integration. In addition, the automatic observation and analysis function Neo Action and the automatic calibration function not only improve efficiency and productivity, but also contribute to the elimination of labor shortages.
Voltage Contrast Observation of the Semiconductor Multi-Chip After SRAM delayering
Schematic diagram of the voltage contrast (VC)
Surface Observation Specimen Holder - SM-71230SOHD
The voltage contrast (VC) is a contrast that occurs in the SEM image by the difference in the conductivity on the surface of the semiconductor device. For example, if a defect occurs in a tungsten plug, the defective plug shows a different contrast compared to the normal plug. This can be used to locate the defect.
5. AES/CP: Visualization of Elements and Distribution by Chemical State in Semiconductor Multi-Chip CP Cross Sections
Cross-sectional analysis is often used in device failure analysis. However, high spatial resolution analysis is needed when analyzing miniaturized and complex devices. AES allows for high spatial and energy resolution analysis of bulk specimens, making performing more detailed failure analysis simpler. As an example, a visualization of the distribution of the elements Si and SiO2 in different chemical states in the SRAM and CMOS region is given below.
Internal Potential Difference Analysis on the pn junction in the Sic Power Semiconductor Diode
The pn junction forms the structure of the board in SiC Power Semiconductor Diodes and holds a vital role in the operation of the device. The performance of this bond is largely dependent on the amount of impurities and the doping process used for this as well as the process in the film formation. Observation can be performed easily with voltage contrast (VC), but there are only limited techniques for detailed analysis of slight differences in dopant concentration with nanometer-order resolution. Using AES, the internal potential difference can be evaluated from the amount of shift in the kinetic energy peak. Here, the SiC power semiconductor pn junction was analyzed. The position of the Si KLL peaks in the p-type region and n-type region differ by 1.3 eV. This energy difference was used to visualize the p-type and n-type regions.
6. EB: Electron Beam Lithography System
EB lithography system is used to draw IC and circuit data designed with EDA (Electronic Design Automation) tools. The patterns are drawn onto glass or wafer substrates using EB lithography system.
JEOL's EB lithography systems are advanced technology, achieving high speed, high precision and high reliability. This EB system uses a variable-shaped 50 kV electron beam and a step-and-repeat stage.
7. Voltage Contrast Imaging by SEM
Voltage Contrast (VC)
Sample: SRAM (3 nm process)
SEM: JSM-IT810<SHL>
Accelerating Voltage: 200 V (no sample bias)
A new electron energy filter suitable for voltage contrast imaging
SEM observation conditions: JSM-IT810<SIL>
Accelerating Voltage: 800 V
Sample: SRAM
8. Elemental Analysis by SEM
High spatial resolution elemental maps using WindowLess EDS
SEM EDS Conditions: JSM-IT800<i>
Accelerating Voltage: 3.5 kV
Sample: IC cross section
9. 3D Observation by FIB-SEM
FIB-SEM System JIB-PS500i
The three dimensional view processing function of FIB-SEM system enables 3D observation
FIB milling condition:
Landing Voltage: 30 kV
Milling Pitch: 5 nm
SEM observation condition:
Landing Voltage: 2 kV
Detector: Backscattered Electron Detector
3D reconstruction software:
"Dragonfly" (Comet Technologies Canada Inc.)
Semiconductor Quick Links
UHR Field Emission SEM
Ultrahigh resolution FE SEM with the most advanced high-resolution analytical technology available today.
InTouchScope™ Field Emission SEM
High resolution, large chamber FE SEM. Compact, versatile Field Emission SEM that offers Smart-Flexible-Powerful performance at a great value.
InTouchScope™ SEM
Versatile research grade SEM.
Benchtop SEM
Incorporates advanced technology and functions that make it simple for users at any skill level to obtain outstanding SEM images and elemental analysis results in minutes.
200kV TEM
Automated, high-throughput S/TEM designed to meet the unique demands of semiconductor device development and manufacturing.
300kV TEM
World's highest resolution in a commercially-available TEM - 300kV.
200kV TEM
Atomic resolution TEM with (Cold-FEG) and next-generation Cs corrector (ASCOR).
200kV TEM
Ultrahigh energy resolution EELS analysis of materials at the atomic scale.
200kV TEM
Advanced analytical, high throughput 200kV S/TEM with Cold Field Emission Gun and dual Silicon Drift Detectors.
200kV TEM
A revolutionary magnetic field-free atomic resolution imaging system.
FIB-SEM
A multipurpose FIB-SEM that delivers the synergy of fast sample preparation, SEM imaging and EDS analysis in a single instrument.
E-Beam Lithography
Direct Write Systems.
E-Beam Lithography
High Throughput Direct Write System.
E-Beam Lithography
Mask/Reticle Fabrication.
Field Emission EPMA
Ultrahigh imaging and analytical resolution with a very high and stable probe current for optimum analytical performance.
LaB6 EPMA
Research grade microprobe.
Field Emission Auger
Field Emission Auger Microprobe, offers the highest spatial resolution available in an Auger microprobe.
Sample Prep
Easy-to-use, sample preparation device for SEM, EPMA, and SAM applications. Broad ion beam polishing using the JEOL cross-section polisher (CP) offers pristine surface preparation with minimal artifacts.
FIB-SEM
Automatic TEM Specimen Preparation System STEMPLING is software for automatic TEM specimen preparation by using FIB.
TEM
3D reconstruction and 3D visualization software applications.