In this report, di(2-ethylhexyl)phthalate, dichloroacetonitrile, and chloral hydrate, which are water quality control target items in water quality testing, were measured by the same column using nitrogen carrier gas. (For He, see MSTips No.325.) As a result, good linearity of the calibration curve and reproducibility at the lower limit of quantification were obtained for all compounds, and are presented in this report.