Analytical Instrument Documents

Structural analysis of polyethylene terephthalates with different crystallinity using JMS-S3000

In this report, we analyzed the oligomer region of the same samples using a high-resolution MALDI-TOFMS JMS-S3000 "SpiralTOF™-plus 2.0" in combination with Kendrick Mass Defect (KMD) analysis.

Off-flavor analysis in natural rubber by using HS-GC/MS/MS

In this application, we report the analysis of off-flavor components in natural rubber by using HS-GC/MS/MS.

End group analysis of poly(methyl methacrylate) using MALDI-TOFMS and GC-TOFMS

In this report, we performed structural analysis of the end groups of poly(methyl methacrylate) by using MALDI-TOFMS and pyrolysis GC-TOFMS in a complementary manner.

Confirmation of the chemical formula of heat/light sensitive compounds using field desorption coupled with high-resolution mass spectrometry

This application note reports the syringe sampling procedure, and measurement results of example compounds that are sensitive to heat and light.

Analysis of mPEG5K-Phosphate using JMS-S3000

In MSTips No. 333, we reported the measurement results of anionic surfactants less than m/z 1000. In this application note, we report the measurement of polyethylene glycol (average molecular weight 5000) having phosphate groups as an end group.

Analysis of Simazine and Thiobencarb by GC-MS method using hydrogen carrier gas

In this report, simazine and thiobencarb, pesticides subject to environmental standards for water pollution, were measured with hydrogen carrier gas. The results show good linearity of the calibration curve and reproducibility at the lower limit of quantification.

Structural Analysis of Polyethylene Terephthalates with Different Crystallinity using Reactive Pyrolysis GC-TOFMS and NMR

In this application note, two types of commercially available PET resins are analyzed by reactive pyrolysis GC-TOFMS and NMR, and the results of analysis to determine whether they are PET or G-PET are reported.

Composition analysis of EO-PO copolymers using JMS-S3000 “SpiralTOF™-plus2.0” and “msRepeatFinder V6”

Here, we will report on the binary copolymer search function newly added to msRepeatFinder V6 and the resulting compositional analysis of EO-PO copolymers using the degree of polymerization plot.

Analysis of di(2-ethylhexyl)phthalate, dichloroacetonitrile and chloral hydrate by GC-MS method using nitrogen carrier gas

In this report, di(2-ethylhexyl)phthalate, dichloroacetonitrile, and chloral hydrate, which are water quality control target items in water quality testing, were measured by the same column using nitrogen carrier gas. (For He, see MSTips No.325.) As a result, good linearity of the calibration curve and reproducibility at the lower limit of quantification were obtained for all compounds, and are presented in this report.

Analysis of di(2-ethylhexyl)phthalate, dichloroacetonitrile and chloral hydrate by GC-MS method using hydrogen carrier gas

In this report, di(2-ethylhexyl)phthalate, dichloroacetonitrile, and chloral hydrate, which are water quality control target items in water quality testing, were measured using hydrogen carrier gas by the same column. (For He, see MSTips No. 325.) As a result, good linearity of the calibration curve and reproducibility at the lower limit of quantification were obtained for all compounds, and are presented in this report.

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