Analytical Instrument Documents

JMS-T2000GC AccuTOF™ GC-Alpha Sensitivity in nitrogen carrier gas ② - EI / FI ion source

We have checked the influences of nitrogen carrier gas on JMS-T2000 GC AccuTOF™ GC-Alpha, and report on MSTips No. 374-376. This report shows the results of the EI (Electron Ionization) / FI (Field Ionization)combination ion source, which is one of the characteristic multi-ionization ion sources of JMS-T2000 GC AccuTOF™ GC-Alpha.

JMS-T2000GC AccuTOF™ GC-Alpha Sensitivity in nitrogen carrier gas ① - EI / PI ion source

We have checked the influences of nitrogen carrier gas on JMS-T2000 GC AccuTOF™ GC-Alpha, and report on MS Tips No. 374-376. This report shows the results of the EI (Electron Ionization) / PI (Photo Ionization) combination ion source, which is one of the characteristic multi-ionization ion sources of JMS-T2000 GC AccuTOF™ GC-Alpha.

High mass-resolution MS imaging using JMS-S3000

In this report, we report the statistical analysis of high-mass resolution MALDI-MSI data of various lipids in biological samples.

Structural analysis of a small molecule using JMS-S3000

SpiralTOF™-plus 2.0 with TOF-TOF option can achieve high precursor ion selectivity due to the long flight path of the spiral ion optics used in the 1st TOFMS. In this application note, we report the structural elucidation of a photodegradation product of reserpine as an example of structural analysis of a component close to a possible interference in mass by MS/MS measurement using the SpiralTOF™-plus 2.0 with TOF-TOF option.

Analysis of oligonucleotides using JMS-S3000

Molecular weight confirmation of synthesized oligonucleotides is important for the quality control of pharmaceuticals. In this report, we used the synthesized oligonucleotide (Table 1) as a sample and measured it with a MALDI-TOFMS.

Differential analysis of coffee aroma compounds using HS GC-QMS and msFineAnalysis iQ

Coffee aroma contains a very large number of components. Therefore, a large number of peaks are observed in TIC chromatogram, and it takes a long time to identify the components of each peak and to analyze differences between samples. In this report, we present the results of differential and integrated analyses performed on coffee aroma components using msFineAnalysis iQ.

Integrated qualitative analysis of fatty acid methyl esters (FAMEs) by msFineAnalysis iQ

We report the results of the integrated qualitative analysis combining library database search and molecular ion confirmation when performing msFineAnalysis iQ.

Elemental Composition Determination of Polymer End Groups Using Accurate Mass

Recently, it has been possible to efficiently overview the information in the mass spectra of complex polymer mixtures using a Kendrick Mass Defect (KMD) analysis software, msRepeatFinder. Determining the elemental composition of the end groups of the polymer series identified in this way is essential for confirming the state of polymer synthesis reactions, quality control of products, and analysis of degradation mechanisms. In this report, we introduce the procedure for determining the elemental compositions of the end groups from the accurate mass information of the polymer.

Additive analysis in lubricating oil by FD method using JMS-T2000GC AccuTOF™ GC-Alpha

In MSTips No. 355, the effectiveness of the FD method in additive analysis was shown using an analysis example of bromine flame retardant in polypropylene products. In this report, we introduce an analysis example of molybdenum dithiocarbamate (MoDTC), which is a friction reducing agent for lubricating oil.

Analysis of brominated flame retardants in polypropylene products by FD method using JMS-T2000GC AccuTOF™ GC-Alpha

This report shows the result of analysis for two types of polypropylene (PP) products. The difference between sample was not found by the pyrolysis method, but a brominated flame retardants was found as a difference by the FD method.

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