rss

JEOL Resources

Documentation in support of your JEOL product.

Rapid Detection and Exact Mass Measurements of Trace Components in an Herbicide

Analytical chemists are often asked to identify trace components in manufactured compounds such as drugs, consumer products, and agricultural chemicals. A common approach to the identification of minor components is to use gas or liquid chromatography coupled with high-resolution mass spectrometry. Although this approach is effective, it may be time consuming and difficult to set up. The AccuTOF with Direct Analysis in Real Time (DART™) provides a rapid solution. The high dynamic range of both source and detector permit the determination of minor components in the presence of a major component. The AccuTOF always provides high resolution data with exact mass measurements and accurate isotope ratios that can provide elemental composition assignments for unknown compounds.

Instantaneous Detection of Explosives on Clothing

The detection of explosives is of vital importance in forensic applications and in preventing criminal or terrorist activity. The analytical detection of explosives on surfaces is normally done by using solvent extractions or wipes and chromatography or chromatography combined with mass spectrometry. This is inefficient because solvent extractions and wipes only result in a partial transfer of material from the surface into the sampling material. Furthermore, the chromatographic analysis can be time-consuming and requires the use of disposable solvents (an environmental concern). The JEOL AccuTOF™ with Direct Analysis in Real Time (DART™) has demonstrated the capability to detect both volatile and involatile explosives on surfaces such as plastic, cloth, concrete, glass, cardboard, metal, and more. No wipes or solvent extractions are required. The method is instantaneous, environmentally friendly, and does not require solvents. An example is shown in this application note.

Detection of Explosives in Muddy Water

The AccuTOF time-of-flight mass spectrometer equipped with Direct Analysis in Real Time (DART™) has been used to detect a wide variety of explosives in or on a variety of materials ranging from solutions to samples deposited on surfaces ranging from ABS plastic to metal, clothing and cardboard. Detection is rapid, specific, and sensitive.

Analytical Instruments Documents

Other Resources

The following resources are available for the JEOL Analytical Instruments:

Media

Corona - Glow Discharge (DART Ion Source)

February 22, 2020
53