Analytical Instrument Documents

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Documentation in support of your JEOL product.

Detection of Lycopene in Tomato Skin

Tomatoes are rich in lycopene, a hydrocarbon antioxidant that is the source of the red coloring in ripe tomatoes. The potential benefits of nutritional antioxidants such as lycopene have received a great deal of attention in the popular media. A piece of tomato skin was placed in front of the DART and the positive-ion mass spectrum was recorded.

Analysis of stobilurins in wheat grains using DART-TOFMS

Strobilurins, systemic pesticides originated from natural fungicidal derivatives, play an important role in control of various plant pathogens. Because of their unique protective properties, significant yield enhancements and longer retention of green leaf tissue, strobilurins have been widely used in agriculture since their introduction on the market in 1992. As other pesticides, these compounds are involved in control and monitoring surveys undertaken by regulation authorities.

Analysis of deoxynivalenol in beer

The AccuTOF-LC time-of-flight mass spectrometer equipped with a DART ion source and AutoDart HTC PAL autosampler, was used for examination of beer in this study. Donprep® immunoaffinity columns (R-Biopharm) was employed for selective isolation of target analyte from the sample. Briefly, 10 mL of beer with added internal standard (13C15-deoxynivalenol, 500 ng/ml) were passed through the cartridge, which was then washed with 5 mL of water. Deoxynivalenol was subsequently eluted with 4.5 mL of methanol. Calibration standards containing deoxynivalenol in the range from 100 to 1500 ng/mL and fixed amount of internal standard (500 ng/mL) were prepared for quantification.

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Corona - Glow Discharge (DART Ion Source)

February 22, 2020
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