Analytical Instrument Documents

Automatic structure analysis software for data acquired by electron ionization and soft ionization Designed specifically for GC-HRTOFMS: AccuTOF™ GC-Alpha

In this work we used msFineAnalysis to compare Vinyl Acetate Resins that were measured by using Pyrolysis (Py)-GC-MS.

In this work, we compare sensitivity levels when using the combination EI/FI and EI/PI ion sources when He and N2 are used as the GC carrier gas.

Catalyzed light olefin oligomerization is widely used in petrochemical industries to produce fuels and chemicals. Light olefins such as propene and butenes are commonly selected as feedstocks. Solid phosphoric acid (SPA) and zeolite are representative acidic catalysts. Both the feedstocks and catalysts have an impact on the product composition. In this study, state-of-the-art instrumentation two-dimensional gas chromatography (GC × GC) coupled photoionization─time of flight mass spectrometry was employed to investigate the composition of dodecene products produced from olefin oligomerization. Information such as the olefin congener distribution, dodecene structural subgroup distribution, and individual dodecene isomers was obtained and utilized in the statistical analyses. By using specific data sets of the product composition, the distinguishment between SPA and zeolite catalysts as well as among the feedstocks was achieved by applying the unsupervised screening approaches (principal component analysis and hierarchical clustering analysis). The potential indicators of catalysts and feedstocks were selected by the feature selection methods (univariate analysis: analysis of variance and multivariate analysis: partial least squares-discriminant analysis).

As polymer materials have become more complex and diverse, the details of their chemical composition have become more critical for the end users. This knowledge allows manufacturers and users to understand the effects of incorporating these polymer materials into their products. Additionally, it is critical to also have tools that can quickly compare two-samples to each other like conventional materials versus alternative materials, new products versus old products, and good products versus defective products.

Gas chromatography combined with high-resolution time-of-flight mass spectrometry (GC-HRTOFMS) is a powerful tool for the analysis of complex mixtures. The AccuTOF GC-Alpha (JMS-T2000GC) mass spectrom-eter is fast, accurate and sensitive with high mass-resolving power and high mass accuracy.

Non-targeted analysis of complex mixtures by GC-HRMS should make use of all of the available data to identify unknowns. An automated data analysis software package combining chromatographic deconvolution with integrated analysis of high-resolution mass spectra for electron ionization (EI) and soft ionization measurements is applied to the identification of trace impurities in a fine chemical (triphenylphosphine).

Various applications on the topics of Materials and Chemistry for the AccuTOF GC Series

Publication containing various applications pertaining to Environment, Food, Flavor, & Fragrance.

Pursuing the ultimate in performance and functionality. The JMS-T2000GC AccuTOF™ GC-Alpha Time-of-Flight Mass Spectrometer takes you to a new world of mass spectrometry, the ultimate GC-MS with superior performance and ease of operation.