Analytical Instrument Documents

Evaluation of Oblique Light-Induced Degradation of Indoor Line Tape by Mass Spectrometry (2)

DEP (Direct Exposure Probe) is a technique in which a sample is directly applied to a platinum filament at the tip of the probe and rapidly heated by applying an electric current to the filament. This method enables rapid ionization while minimizing thermal decomposition of the sample, thus requiring little to no complex sample pretreatment and making it suitable for the analysis of nonvolatile substances or those prone to thermal decomposition. In this study, therefore, a direct introduction method using DEP was applied, and the results of rapid qualitative analysis of organic pigments contained in the pigmented layer of an indoor line tape are reported.

Evaluation of Oblique Light-Induced Degradation of Indoor Line Tape by Mass Spectrometry (1)

In this study, a case was examined in which indoor line tape used for approximately eight months exhibited a degradation phenomenon where the color of the pigmented layer disappeared due to the influence of oblique light. The objective was to evaluate this oblique light-induced degradation and to clarify its underlying causes. For the evaluation, qualitative analysis of the substrate layer and adhesive layer constituting the tape was first carried out using the direct EGA-MS (Evolved Gas Analysis–Mass Spectrometry) method. This technique enabled direct detection of thermally decomposed products from each constituent layer, allowing for characterization of the material composition.

Ion Exchange Resin Analysis by using Pyrolysis-GCxGC-MS

In this study, pyrolysis (Py)/GCxGC/HR-TOFMS system was applied to investigate the pyrolysis products of Vinylpyridine and Divinylbenzene copolymer as the ion exchange resin sample.

Ethylene Propylene Diene Monomer Rubber Analysis by using Pyrolysis-GCxGC-MS

In this study, pyrolysis(Py)/GCxGC/HR-TOFMS system was applied to investigate the pyrolysis products of Ethylene-propylene–diene rubber (EPDM).

Analysis of a drug in urine by JMS-S3000

In this report, we analyzed methylephedrine, a phenethylamine compound, in common cold medicines as an application to the field of forensic chemistry.

Measurement examples of organic pigments using Laser Desorption/Ionization (LDI) and Field Desorption (FD)

In this work, commercially available organic pigments were analyzed using JMS-S3000 SpiralTOF™ and JMS-T200GC AccuTOF™ GCx-plus. Measurements were performed by matrix-free LDI (Laser Desorption Ionization) on the JMS-S3000 and by FD (Field Desorption) on the JMS-T200GC. Because good results were obtained with both methods, we report them here.

Analysis of medicinal properties in a combination cold remedy by using JMS-S3000

In this report, we will discuss the analysis of medicinal components in a combination cold remedy.

MALDI-ISD Measurements Using Both the SpiralTOF Mode and the LinearTOF Mode of JMS-S3000 “SpiralTOF™”

Matrix-assisted laser desorption/ionization (MALDI) combined with in-source decay (ISD) is a useful tool for doing top-down sequencing of intact proteins. In this work, we measured and compared the ISD fragment ions generated for several proteins using the high resolution MALDI- Spiral mode and the high sensitivity MALDI-Linear mode available on the JEOL SpiralTOF MALDI-MS system.

High Sensitivity Analysis of intact Proteins Using Linear TOF

In this work, we demonstrate the measurement of intact proteins by using the Linear TOF option for the JEOL SpiralTOF system.

Rapid Confirmation of Synthetic Compounds Using DART™ –Direct Mass Spectrometric Analysis from NMR Sample Tubes

We report an application related to synthetic compound confirmation that combines nuclear magnetic resonance (NMR), which is indispensable for structural analysis of organic compounds, and mass spectrometry by DART.

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